Synthesis and Characterization of Osmium-Containing Silsesquioxanes: High-Yield Routes to {Os3(CO)10(m-H)[(m-O)Si7O10(c-C6h11)7]} and the New Clusters {Os3(CO)10(m-H)[(m-O)Si7O9(OH)2(c-C6h11)7]}, {[Os3(CO)10(m-H)]2(m-O)2Si7O9(OH)(c-C6h11)7]}, {Os3(CO)10(m-H)[(m-O)Si8O11(OH)(c-C6h11)8]}, and {[Os3(CO)10(m-H)]2(m-O)2Si8O11(c-C6h11)8]}

doi 10.1021/om060844c.s004
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